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L& Notes I Packing List Michigan Notes Farrah ƻ Farrah's \
Root Notes
Roots E Litter Notes " Litter 2005 ai y Questions for Farrah: Will we see this "bottle?" number somewhere? Can you add the matrix for the three reagent blanks? Samples 100-121 were all numbered and sent to Michigan by Bill because he thought they were all standards and blanks, and these were first priority for Joel's lab to rerun.4 Farrah figured out that they were not all standards.5 Farrah, are we interested in re-running these blanks? "Farrahs" samples include the tissue standards that are highest priority for analysis, but also other samples that were sent by mistake. sent, but don't analyzeo There is no reason to re-run her other samples at this time. They have been labeled "sent, but don't analyze". These are probably even lower priority than "sent, but don't analyze yet" (the ones we digested with the roots were suspicious outliers).w Bottom line for Joel: First priority, all systems are awaiting the analysis of Farrah's tissue standards, 9 samples. 9 Ruth and BB are waiting for the root samples, 87 samples.A Everyone and noone is waiting for the litter samples, 48 samples.{ This list also contains some samples of Farrah's that we digested, probably ones that looked like outliers in her data set.q It's not important to run these if we discover that her digestions were fine, but her ICP analyses were not good._ First priority is to run her standards and see if Joel's ICP results give the certified values. not sent
Sample wt. sent, but don't analyze yet On the "Packing List" there are 3 sample numbers that were not in fact sent to Michigan (they were numbered before we realized we shouldn't send them). Details on "Litter Notes" page.T There are also 13 samples on the packing list labeled "sent, but don't analyze yet."u These are samples of Farrah's that didn't look good in her chemistry results, so we re-digested her archived samples.n Later we realized that we could send you her digested solutions to see if you get better results than she did. We decided that the first priority would be to re-run her digested tissue standards, to see if you get the certified values where she did not.P If so, we needn't repeat the digestions, only the ICP analysis of the solutions." Notes reorganized by Ruth, 3/23/08 Bottle? Digestion ID Description ID Volume Matrix APPLE 4 ml HNO3 + 2 ml HCl Sample C4 56 BE LV
C6 C RM BR C2 45 YB BR C4 59 WB BR C6 37 BE BR C4 47 YB WD C2 40 RM WD Sample
C6 3 BE BK C6 37 BE BK C1 26 WB BK FAT 521 10 ml 6N HCl FAT 545 FAT 569 Notes by Ruth, 3/23/08 LT 138 LT 139 LT 140 LT 141 LT 142 LT 143 LT 144 LT 145 LT 146 LT 147 LT 148 SAMPLE DOES NOT EXIST LT 149 LT 150 LT 151 LT 152 LT 153 LT 154 LT 155 LT 156 LT 157 FOLIAGE LT 158 LT 159 Tissue Wt. Mich#" Litter 2006 Rerun for all elements Volume was 50 ml.
Notes by RuthH Roots collected in Summer 04, digested in Summer 07, in need of analysis Pit=Pit Column headingsL Bill assigned numbers sequentially to vials to ship to Michigan for analysis This list combines all the sample sets that have been sent to Michigan from ESF. So the column headings don't always make sense.: See the individual "Notes" pages for better documentation.e Unfortunately, they were assigned "Michigan numbers" before we decided they shouldn't go to Michigan. 3/23/08 Ruth Farrah's list also included these two entries, to tell us not to think we were missing samples, because the LT numbers continue after these.H T h e y w e r e a s s i g n e d M i c h i g a n n u m b e r s , b u t w e c o u l d n ' t h a v e s e n t a n y t h i n g & ] BILL, CAN WE FORGET ABOUT 173 AND 174, AND START NUMBERING THERE IF WE SEND ANY MORE SAMPLES?5 FARRAH, WE NEED TO KNOW WHAT YOU DIGESTED THESE IN. Q One of the 6 "intensive" sites at Bartlett in which roots were collected in 2004.. There were 3 soil pits excavated at each site.R The soil pits were excavated in depth increments. Roots came from this increment." Roots were sorted by diameter (mm)- C=composited sample (from multiple soil pits). Only P was run on the ICP for these samples. w Im not sure why there are no standards with this set, but I can't find any data on them, so it looks there aren't any. by e-mail 1/25/2008 FarrahU Tarp indicates one out of three tarps that were set out in each stand (A, B and C). l When litter was sorted, it was sorted by species and then collated by species and tarp it was collected on. The following samples were not sent to Joel but were found with the litter samples. Farrah was running three orphaned tissue samples for her thesis project. We will keep them in Syracuse.0 These are Bartlett litter samples from Fall 2005? "Packing List Michigan" includes everything we've sent to Joel.P At the top are the digested root samples and re-runs of Farrah's tissue samples.B "Litter 2005" describes the samples we are sending today, 2/13/08. Sample weight is in column F. Site Depth Diameter C2 10-30 5-10 0-1 30-50 dup Oa C4 C9 C1 SM branches bark C6 wood 0-10 10-20 C8 Blank C dup C Notes Pit dup=Duplicate sample C=composited sample RM Leaves PC LF1 YB BE LF4 WB
Standard 2006
Standard 2004* Diameter=Root diameter (mm) or tissue type Mich #! Depth=Root depth (cm) or species Sample ID Tarp Species LT 107 ** BARK SM 80 LT 108 SM 97 LT 109 B LITTER PB LT 110 A LT 111 LT 112 LT 113 LT 114 LT 115 LT 116 LT 117 LT 118 LT 119 LT 120 LT 121 LT 122 LT 123 LT 124
REAGENT BLANK LT 125 LT 126 LT 127 LT 128 LT 129 LT 130 LT 131 LT 132 LT 133 LT 134 LT 135 LT 136 LT 137
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